|
Iest. |
d(meas.) (Å) |
d(calc.) (Å) |
hkl |
|
Iest. |
d(meas.) (Å) |
d(calc.) (Å) |
hkl |
|
|
70 |
8.547 |
8.607 |
200 |
|
3 |
2.227 |
2.233 |
 22 |
|
20 |
6.475 |
6.468 |
110 |
|
3 |
2.154 |
2.156 |
330 |
|
30 |
4.796 |
4.79 |
 11 |
|
|
|
2.152 |
800 |
|
15 |
4.467 |
4.437 |
111 |
|
5 |
2.116 |
2.119 |
13 |
|
5b |
3.453 |
3.489 |
020 |
* |
10 |
2.065 |
2.066 |
711 |
|
|
|
3.43 |
311 |
|
20 |
1.97 |
1.97 |
602 |
| * |
100 |
3.275 |
3.277 |
002 |
|
|
|
1.969 |
422 |
| * |
10 |
3.082 |
3.08 |
021 |
* |
50 |
1.878 |
1.878 |
 23 |
| * |
80 |
2.993 |
2.992 |
21 |
* |
15 |
1.848 |
1.849 |
 21 |
| * |
80 |
2.873 |
2.869 |
600 |
* |
20 |
1.745 |
1.745 |
040 |
| * |
20b |
2.82 |
2.816 |
221 |
* |
30 |
1.686 |
1.686 |
041 |
| * |
10 |
2.712 |
2.71 |
420 |
|
10 |
1.642 |
1.647 |
513 |
| * |
30 |
2.625 |
2.626 |
21 |
|
|
|
1.646 |
04 |
|
|
|
2.415 |
 02 |
|
5 |
1.603 |
1.604 |
423 |
|
50b |
2.404 |
2.399 |
421 |
|
15 |
1.563 |
1.568 |
 21 |
|
|
|
2.395 |
22 |
|
|
|
1.566 |
04 |
|
15 |
2.319 |
2.331 |
 11 |
* |
20 |
1.541 |
1.541 |
23 |
|
|
|
2.319 |
710 |
|
|
|
|
|
|
|
114.6 mm Debye-Scherrer powder camera; Cu radiation, Ni filter ( Cu-K = 1.54178 Å) |
| Intensities estimated visually; b = broad line |
| Not corrected for shrinkage and no internal standard; * = lines used for unit-cell refinement |
| Indexed with a = 17.580, b = 6.979, c = 6.693 Å, ß = 101.71° |
|
